7-甲氧基-2-苯基喹啉合成路线 (共 13 条)
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene T=80°C; 12 h;
参考文献
Panda, Kausik; Siddiqui, Iffat; Mahata, Pranab K.; Ila, Hiriyakkanavar; Junjappa, Hiriyakkanavar
Synlett, 2004 , # 3 p. 449 - 452
反应条件
1: 78 percent / glac. AcOH / Heating 2: 74 percent / (PPh3)2NiCl2 / diethyl ether; benzene / 12 h / 80 °C View Scheme
参考文献
Borsche; Wagner-Roemmich
Justus Liebigs Annalen der Chemie, 1940 , vol. 544, p. 280,284
反应条件
palladium on activated charcoal; Lindlar's catalyst; ethanol Hydrogenation;
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
反应条件
1: phosphorus (V)-chloride 2: toluene / Erhitzen des Reaktionsprodukts auf 150-170grad 3: aqueous NaOH 4: 360 °C / Im Vakuum 5: phosphoryl chloride 6: palladium/calcium carbonate; ethanol / Hydrogenation View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
反应条件
1: phosphoryl chloride 2: palladium/calcium carbonate; ethanol / Hydrogenation View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
反应条件
1: 360 °C / Im Vakuum 2: phosphoryl chloride 3: palladium/calcium carbonate; ethanol / Hydrogenation View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
反应条件
1: aqueous NaOH 2: 360 °C / Im Vakuum 3: phosphoryl chloride 4: palladium/calcium carbonate; ethanol / Hydrogenation View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
反应条件
1: toluene / Erhitzen des Reaktionsprodukts auf 150-170grad 2: aqueous NaOH 3: 360 °C / Im Vakuum 4: phosphoryl chloride 5: palladium/calcium carbonate; ethanol / Hydrogenation View Scheme
参考文献
Elderfield et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1272,1275
参考文献
Schneider; Pothmann
Chemische Berichte, 1941 , vol. 74, p. 471,479
反应条件
1: mercury 2: diethyl ether View Scheme
参考文献
Schneider; Pothmann
Chemische Berichte, 1941 , vol. 74, p. 471,479