2,4,6-三甲氧基苄硫醇合成路线 (共 3 条)
反应条件
1: With toluene-4-sulfonic acid; thiourea in acetonitrile 2: With sodium hydroxide Further stages.;
参考文献
Vetter, Stefan
Synthetic Communications, 1998 , vol. 28, # 17 p. 3219 - 3223
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 0.166667 h; 2: With sodium hydrogencarbonate in dichloromethane; water
参考文献
Dyer, Frank Brock; Park, Chung-Min; Joseph, Ryan; Garner, Philip
Journal of the American Chemical Society, 2011 , vol. 133, # 50 p. 20033 - 20035
反应条件
sodium hydroxide in ethanol; water
T=0 - 20°C; 4 h;
参考文献
PFIZER PRODUCTS INC.
Patent: WO2004/11461 A1, 2004 ;
Location in patent: Page 31 ;
WO 2004/011461 A1