2,2'-二硫双(5-硝基吡啶)合成路线 （共 6 条）
反应条件
hydrogenchloride; ammonium hydroxide; chlorine 1.) -15 deg C to -25 deg C, 15 min, 2.) RT, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Medicinal Chemistry, , vol. 23, # 12 p. 1376 - 1380
反应条件
1: methanol; potassium hydrogensulfide 2: water; hydrogen peroxide View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 487, p. 105,115
反应条件
water; dihydrogen peroxide
参考文献
Justus Liebigs Annalen der Chemie, , vol. 487, p. 105,115
反应条件
anhydrous trisodium citrate; TiCl3 in ethanol; water; acetic acid pH 4.5 to 6.O;
参考文献
Akers, Hugh A.; Vang, Meng C.; Updike, Tracie D.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1364 - 1366
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in chloroform
参考文献
Nyoni, Dubekile; Lobb, Kevin A.; Kaye, Perry T.; Caira, Mino R.
Arkivoc, 2012 , vol. 2012, # 6 p. 245 - 252
参考文献
Pfizer Inc.
Patent: US6407120 B1, 2002 ;
Location in patent: Page column 9-10 ;
US 6407120 B1
