1: nitromethane With 1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide T=0°C; 0.166667 h; 2: benzenesulphinic acid sodium salt With iodine in N,N-dimethyl-formamide T=20°C; 1 h;
1: nitromethane Inert atmosphere; 2: benzenesulphinic acid sodium salt With iodine Inert atmosphere; 3: With hydrogenchloride in water Inert atmosphere;
参考文献
Journal of Physical Organic Chemistry, , vol. 22, # 4 p. 337 - 342
