Eisch, John J.; Piotrowski, Andrzej M.; Aradi, Allen A.; Krueger, Carl; Romao, Maria J.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1985 , vol. 40, # 5 p. 624 - 635
in diethyl ether under N2 or Ar, Ph4C4Li2 suspended in anhyd. Et2O at -78°C, PhBCl2 added, warmed to 20°C with stirring, stood for 2 h at 20-25°C; evapd. in vac., anhyd. deoxygenated toluene added, shaked at 60-70°C, cooled sepd. toluene exts.; elem. anal.;
参考文献
Eisch,J.J.; Galle,J.E.; Kozima,S.
Journal of the American Chemical Society, 1986 , vol. 108, p. 379
in tetrahydrofuran; diethyl ether soln. of dilithio reagent (ether) was dropwise added to soln. of diphenyltin dichloride (THF), 2 h, stirred under N2 at reflux; ether was remeved in vac., dichloromethane was added, and filtered, concd. and abs. ethanol was added, pptd. by cooling with dry ice; recrystd.from dichloromethane-ethanol; isolated the butadienyl-diphenyltin dichloride; elem. anal.;
参考文献
Gustavson, W. A.; Principe, L. M.; Rhee, W.-Z. Min; Zuckerman, J. J.
Journal of the American Chemical Society, 1981 , vol. 103, # 14 p. 4126 - 4131
