4-二甲氨基苯基硫代异氰酸酯合成路线 （共 23 条）
反应条件
triethylamine in tetrahydrofuran T=25°C; 12 h;
参考文献
Wilcox, Craig S.; Kim, Eun-il; Romano, David; Kuo, Lung Huang; Burt, Arthur L.; Curran, Dennis P.
Tetrahedron, 1995 , vol. 51, # 2 p. 621 - 634
反应条件
sodium hydroxide in dichloromethane T=20°C; 1 h;
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
sodium hydroxide in dichloromethane T=0 - 20°C; 21 h;
参考文献
Li, Zheng-Yi; Ma, Hong-Zhao; Han, Chen; Xi, Hai-Tao; Meng, Qi; Chen, Xin; Sun, Xiao-Qiang
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-F0228-OP, p. 1667 - 1674
反应条件
1: With triethylamine in methanol T=0 - 5°C; 2: With bis(trichloromethyl) carbonate in chloroform T=0°C; 4 h; Further stages.;
参考文献
Chaskar; Yewale; Bhagat; Langi
Synthetic Communications, 2008 , vol. 38, # 12 p. 1972 - 1975
反应条件
sodium hydrogencarbonate in dichloromethane T=0°C; 0.5 h;
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 6 p. 936 - 953
参考文献
Journal of the American Chemical Society, , vol. 75, p. 2364
反应条件
1: NH3 / 0.5 h 2: lead sulfide / H2O / Heating View Scheme
参考文献
Journal of Physical Organic Chemistry, , vol. 15, # 8 p. 570 - 575
反应条件
in toluene 30 h; Heating;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 33, # 3 p. 355 - 360
反应条件
sodium hydrogencarbonate in chloroform 0.5 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 7 p. 915 - 918
反应条件
in dichloromethane T=20°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 12 p. 3916 - 3920
