1,2-二(4-乙氧基苯基)-1,2-乙烷二酮合成路线 (共 10 条)
参考文献
Schoenberg; Kraemer
Chemische Berichte, 1922 , vol. 55, p. 1189
反应条件
samarium; potassium iodide; copper(l) chloride in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Liu, Yongjun; Wang, Hui; Fu, Yulong; Qi, Yan; Yang, Kuiwei
Synthetic Communications, 2014 , vol. 44, # 2 p. 259 - 266
反应条件
AlCl3, aluminium chloride in dichloromethane
Friedel Crafts reaction; 6 h; RefluxLarge scale reaction;
参考文献
Cao, Xingbo; Jin, Feng; Li, Ying-Feng; Chen, Wei-Qiang; Duan, Xuan-Ming; Yang, Lian-Ming
New Journal of Chemistry, 2009 , vol. 33, # 7 p. 1578 - 1582
反应条件
sodium hydroxide; thiamine chloride hydrochloride in ethanol; water
72 h;
参考文献
Hischer, Tanja; Gocke, Doerte; Fernandez, Maria; Hoyos, Pilar; Alcantara, Andres R.; Sinisterra, Jose V.; Hartmeier, Winfried; Ansorge-Schumacher, Marion B.
Tetrahedron, 2005 , vol. 61, # 31 p. 7378 - 7383
反应条件
1.1: KOH / ethanol
2.1: Mg / tetrahydrofuran
2.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran
3.1: SeO2; 90 percent aq. AcOH; H2SO4
View Scheme
参考文献
Horie; Takagi; Hasebe; Ozawa; Ohta
Journal of Materials Chemistry, 2001 , vol. 11, # 4 p. 1063 - 1071
反应条件
1.1: Mg / tetrahydrofuran
1.2: dichloro[1,3-bis(diphenylphosphino)ethane]nickel(II) / tetrahydrofuran
2.1: SeO2; 90 percent aq. AcOH; H2SO4
View Scheme
参考文献
Horie; Takagi; Hasebe; Ozawa; Ohta
Journal of Materials Chemistry, 2001 , vol. 11, # 4 p. 1063 - 1071
反应条件
1: AlCl3; carbon disulfide / -5 °C
2: SeO2; acetic acid
View Scheme
参考文献
Nagano
Journal of Organic Chemistry, 1957 , vol. 22, p. 817
反应条件
sodium hydroxide
1.5 h; Heating;
参考文献
Cannon, Jack R.; Patrick, Vincent A.; White, Allan H.
Australian Journal of Chemistry, 1989 , vol. 42, # 10 p. 1631 - 1646
反应条件
selenium(IV) oxide; sulfuric acid; acetic acid
参考文献
Horie; Takagi; Hasebe; Ozawa; Ohta
Journal of Materials Chemistry, 2001 , vol. 11, # 4 p. 1063 - 1071
反应条件
hydrogenchloride; carbon disulfide; aluminium trichloride
man zerlegt das Reaktionsprodukt mit verd. Salzsaeure;
参考文献
Vorlaender
Chemische Berichte, 1911 , vol. 44, p. 2465