林可霉素 2,7-二乙酸酯合成路线 （共 119 条）
反应条件
in pyridine 12 h; Heating;
参考文献
Organic Mass Spectrometry, , vol. 24, p. 903 - 908
反应条件
(i) nBuLi, Et2O, THF, hexane, PE, (ii) (heating); Multistep reaction;
参考文献
Chemische Berichte, , vol. 99, p. 680 - 688
参考文献
Justus Liebigs Annalen der Chemie, , vol. 279, p. 318
反应条件
in acetonitrile Irradiationdifferent solvents, in absence and presence of O2; Mechanism;
参考文献
Journal of the Chemical Society, Faraday Transactions, , vol. 88, # 10 p. 1385 - 1390
参考文献
Justus Liebigs Annalen der Chemie, , vol. 463, p. 208
反应条件
1,4-dioxane; Pd-BaSO4 Hydrogenation;
参考文献
Weygand; Siebenmark
Chemische Berichte, 1940 , vol. 73, p. 765,769
反应条件
tris[N-(tert-butyl)(3,5-dimethylphenyl)amido]molybdenum(VI) propylidyne; tris(2-hydroxy-5-nitro-benzyl)amine in tetrachloromethane T=40°C; 7 h; Inert atmosphere;
参考文献
Jyothish, Kuthanapillil; Zhang, Wei
Angewandte Chemie - International Edition, 2011 , vol. 50, # 15 p. 3435 - 3438
反应条件
in tetrahydrofuran Irradiation (UV/VIS); (Ar) soln. Cr complex and alkyne in THF was irradiated with Hg/Xe arc lamp (400-550 W) atb 210-600 nm for 5 h at room temp.; volatiles were removed in vacuo, residue was extd. with hexane, soln. was decanted and stored at -60°C overnight, soln. was filtered and evapd. in vacuo; elem. anal.;
参考文献
Braunschweig, Holger; Herbst, Thomas; Rais, Daniela; Ghosh, Sundargopal; Kupfer, Thomas; Radacki, Krzysztof; Crawford, Andrew G.; Ward, Richard M.; Marder, Todd B.; Fernandez, Israel; Frenking, Gernot
Journal of the American Chemical Society, 2009 , vol. 131, # 25 p. 8989 - 8999
反应条件
1: 81 percent / [Co2(CO)8] / dioxane / 24 h / 100 °C 2: 92 percent / BBr3 / CH2Cl2 / 18 h / 20 °C View Scheme
参考文献
Morisue, Mitsuhiko; Suzuki, Wataru; Kuroda, Yasuhisa
Dalton Transactions, 2011 , vol. 40, # 39 p. 10047 - 10054
反应条件
iodine in dimethyl sulfoxide T=145°C; 2 h;
参考文献
Yusubov, M. S.; Chi, Ki Whan; Krasnokutskaya, E. A.; Vasil'eva, V. P.; Filimonov, V. D.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 11 p. 1503 - 1506
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 11 p. 1675 - 1678
