林可霉素 2,7-二乙酸酯合成路线 （共 119 条）
反应条件
lithium perchlorate in acetonitrile 9 h; anodic oxidation;
参考文献
Tetrahedron, , vol. 47, # 4/5 p. 799 - 808
参考文献
Tan, Kristine J.; Wille, Uta
Chemical Communications, 2008 , # 46 p. 6239 - 6241
反应条件
lithium perchlorate in acetonitrile 9 h; electro-oxidation, graphite plate electrode;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 445 - 446
反应条件
in various solvent(s) 9 h; anodic oxidation; Mechanism;
参考文献
Tetrahedron, , vol. 47, # 4/5 p. 799 - 808
反应条件
hydrogenchloride; zinc(II) chloride in dichloromethane 0.5 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 116, # 2 p. 777 - 797
反应条件
sulfuric acid; water; acetic acid T=40 - 50°C;
参考文献
Eckart, Klaus; Helmut, Schwarz; Kobayashi, Shinjiro; Taniguchi, Hiroshi
Organic Mass Spectrometry, 1982 , vol. 17, # 9 p. 457 - 458
反应条件
in petroleum ether stirred under a stream of N2 at 23°C for 24h; chromy. on a silica gel;;
参考文献
Krone-Schmidt, W.; Sieber, W.J.; Boag, N.M.; Knobler, N.M.; Kaesz, H.D.
Journal of Organometallic Chemistry, 1990 , vol. 394, # 1/3 p. 433 - 454
反应条件
N-iodo-succinimide; trimethylsilylazide in 1,2-dichloro-ethane; acetonitrile T=20 - 70°C; 3 h; ConcentrationSolventTemperatureTimeReagent/catalyst;
参考文献
Okamoto, Noriko; Ishikura, Minoru; Yanada, Reiko
Organic Letters, 2013 , vol. 15, # 11 p. 2571 - 2573
反应条件
1,4-dioxane; Pd-BaSO4
Hydrogenation;
参考文献
Kuroda; Dekura; Sato; Mori
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4139 - 4146
参考文献
Coleman; Holst; Maxwell
Journal of the American Chemical Society, 1936 , vol. 58, p. 2310
