反应条件
hydrogenchloride; methanol; benzene; bis-triphenylphosphine-palladium(II) chloride in methanol; diethyl ether; benzene N2 atmosphere; evapn. of soln. p-MeOC6H4MgBr (65°C), addn. of benzene, (PPh3)2PdCl2 and carborane, heating (60-65°C, 40 h), addn. of benzene, addn. of MeOH and HCl (0°C); evapn., extn. (benzene/hexane, 60°C), drying, dissolving (benzene), addn. of BuLi in hexane, heating (60°C, 1 h), pptn., filtration off, washing (benzene), drying (over CaCl2), sublimation (120-170°C, 1 mm), recrystn.; elem. anal.;
参考文献
Kovredov, A. I.; Shaugumbekova, Zh. S.; Petrovskii, P. V.; Zakharkin, L. I.
Journal of General Chemistry USSR (English Translation), 1989 , vol. 59, p. 537 - 540
Zhurnal Obshchei Khimii, 1989 , vol. 59, p. 607 - 611
