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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4,4-二甲氧基联苯
合成路线
（共 589 条）
33397-21-6
+
103-80-0
氯化苯乙酰
→
反应条件
1023-17-2
4-甲氧基-2-苯基苯乙酮
+
2132-80-1
4,4-二甲氧基联苯
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
33397-21-6
+
53056-20-5
2,4-二氯苯乙酰氯
→
反应条件
2132-80-1
4,4-二甲氧基联苯
+
153529-19-2
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran T=80°C; 3 h; Schlenk tubeInert atmosphere;
参考文献
Rao, Maddali L.N.; Giri, Somnath; Jadhav, Deepak N.
Tetrahedron Letters, 2009 , vol. 50, # 45 p. 6133 - 6138
696-62-8
4-碘苯甲醚
+
22702-76-7
氯(二甲基)苯基锗烷
→
反应条件
613-37-6
4-甲氧基联苯
+
2132-80-1
4,4-二甲氧基联苯
反应条件
tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride in tetrahydrofuran; water; toluene T=100°C; 15 h; Inert atmosphere;
参考文献
Pitteloud, Jean-Philippe; Zhang, Zun-Ting; Liang, Yong; Cabrera, Laura; Wnuk, Stanislaw F.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8199 - 8212
1003-09-4
2-溴噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
42545-43-7
2-(4-甲氧苯基)噻吩
+
2132-80-1
4,4-二甲氧基联苯
+
492-97-7
2,2'-联二噻吩
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: thien-2-yl bromide With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
5370-25-2
2-乙酰基-5-溴噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
13918-67-7
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 1-(5-bromo-thien-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
30955-94-3
2-乙酰基-5-碘噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
13918-67-7
+
18494-73-0
5,5-二乙酰基-2,2-联噻吩
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 1-(5-iodothiophen-2-yl)ethanone With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
31161-46-3
2-溴-5-苯甲酰基噻吩
+
13139-86-1
3-甲基-CBS-氧硼啶
→
反应条件
13858-69-0
+
2132-80-1
4,4-二甲氧基联苯
反应条件
1: 4-methoxyphenyl magnesium bromide With bismuth(III) chloride 2: 2-benzoyl-5-bromothiophene With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Banerjee, Debasis; Dhanorkar, Ritesh J.
Synlett, 2011 , # 9 p. 1324 - 1330
4786-20-3
2-丁烯腈
+
696-62-8
4-碘苯甲醚
→
反应条件
103927-75-9
+
2132-80-1
4,4-二甲氧基联苯
反应条件
N,N-dicyclohexylmethylamine; palladium diacetate in N,N-dimethyl acetamide T=85°C; Heck Reaction; 16 h;
参考文献
Tetrahedron Letters, , vol. 54, # 16 p. 2042 - 2045
104-92-7
4-溴苯甲醚
+
348-51-6
2-氯氟苯
→
反应条件
2132-80-1
4,4-二甲氧基联苯
+
388-82-9
2,2-二氟联苯
+
72093-47-1
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI in tetrahydrofuran; benzene T=63°C; 2.75 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
104-92-7
4-溴苯甲醚
+
625-98-9
3-氯氟苯
→
反应条件
396-64-5
3,3'-二氟联苯
+
2132-80-1
4,4-二甲氧基联苯
+
72093-48-2
3-氟-4-甲氧基联苯
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI in tetrahydrofuran; benzene T=63°C; 1.25 h; Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
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