Board of Governors for Higher Education, State of Rhode Island and Providence Plantations
Patent: US8334404 B2, 2012 ;
Location in patent: Page/Page column 2 ;
in further solvent(s) Kinetics; byproducts: C2H5F, (C2H5)2O, OPF2(OC2H5); thermal decomposition of LiPF6 soln. in diethylcarbonate at 85-100 °C for 1-4 weeks; also OPF(OC2H5)2 and C2H4 obtained; detd. by chromy.;
参考文献
Campion, Christopher L.; Li, Wentao; Lucht, Brett L.
Journal of the Electrochemical Society, 2005 , vol. 152, # 12 p. A2327-A2334
in further solvent(s) Kinetics; byproducts: OPF2OR, OPF(OR)2, OPF(OH)(OR); thermal decomposition of LiPF6 soln. in ethylenecarbonate at 240 °C for 20-60 min; also OPF2(OC2H5)nF obtained; residual solid extd. with Et2O, evapd. to dryness, redisoolved in d6-benzene; detd. by chromy.;
参考文献
Campion, Christopher L.; Li, Wentao; Lucht, Brett L.
Journal of the Electrochemical Society, 2005 , vol. 152, # 12 p. A2327-A2334
in further solvent(s)
Kinetics; byproducts: OPF2OR, OPF(OR)2, OPF(OH)(OR); thermal decomposition of LiPF6 soln. in ethylenecarbonate at 240 °C for 20-60 min; also OPF2(OC2H5)nF obtained; residual solid extd. with Et2O, evapd. to dryness, redisoolved in d6-benzene; detd. by chromy.;
参考文献
Campion, Christopher L.; Li, Wentao; Lucht, Brett L.
Journal of the Electrochemical Society, 2005 , vol. 152, # 12 p. A2327-A2334
in further solvent(s)
Kinetics; byproducts: C2H5F, (C2H5)2O, OPF2(OC2H5); thermal decomposition of LiPF6 soln. in diethylcarbonate at 85-100 °C for 1-4 weeks; also OPF(OC2H5)2 and C2H4 obtained; detd. by chromy.;
参考文献
Campion, Christopher L.; Li, Wentao; Lucht, Brett L.
Journal of the Electrochemical Society, 2005 , vol. 152, # 12 p. A2327-A2334
