2-环己基异吲哚-1,3-二酮合成路线 （共 42 条）
反应条件
1: in N,N-dimethyl acetamide
T=20°C; 24 h;
2: in N,N-dimethyl acetamide; xylene
T=140°C; 48 h;
参考文献
Li, Xiuru; Zhan, Jie; Li, Yuesheng
Macromolecules, 2004 , vol. 37, # 20 p. 7584 - 7594
反应条件
copper(l) iodide; di-tert-butyl peroxide; 4,7-Dimethoxy-1,10-phenanthroline in benzene
T=100°C; 24 h; Inert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
参考文献
Kreher, Richard P.; Hennige, Hans; Jelitto, Frank; Preut, Johannes
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 9 p. 1132 - 1148
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate
T=130°C; 9 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
European Journal of Organic Chemistry, 2011 , # 33 p. 6719 - 6724
反应条件
1H-imidazole; N,N-dimethyl-formamide in neat (no solvent)
T=150°C; 3 h;
参考文献
Neves Filho, Ricardo A. W.; Palm-Forster, Mieder A. T.; De Oliveira, Ronaldo N.
Synthetic Communications, 2013 , vol. 43, # 11 p. 1571 - 1576
反应条件
in acetonitrile
T=180°C; 1.5 h; Inert atmosphereSealed tubeMicrowave irradiation; Reagent/catalystTemperatureTime;
参考文献
Chorell, Erik; Chorell, Elin
European Journal of Organic Chemistry, 2013 , # 33 p. 7512 - 7516
反应条件
di-tert-butyl peroxide; (phthalimidato)copper(1,10-phenanthroline) in acetonitrile
T=100°C; 24 h; GloveboxInert atmosphere;
参考文献
Tran, Ba L.; Li, Bijie; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2014 , vol. 136, # 6 p. 2555 - 2563
反应条件
4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane in tetrahydrofuran
0.166667 h;
参考文献
Pasquini, M. A.; Goaller, R. Le; Pierre, J.L.
Tetrahedron, 1980 , vol. 36, # 82 p. 1223 - 1226
反应条件
sodium hydroxide in water; acetonitrile
1.5 h; Irradiation;
参考文献
Suau, Rafael; Garcia-Segura, Rafael; Sanchez-Sanchez, Cristobal; Perez-Inestrosa, Ezequiel; Pedraza, Ana Maria
Tetrahedron, 2003 , vol. 59, # 16 p. 2913 - 2919
反应条件
sodium hydroxide in water; acetonitrile
Irradiation; Yields of byproduct given;
参考文献
Suau, Rafael; Garcia-Segura, Rafael; Sanchez, Cristobal; Pedraza, Ana Maria
Tetrahedron Letters, 1999 , vol. 40, # 10 p. 2007 - 2010
