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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
213596-33-9
合成路线
（共 94 条）
619-42-1
对溴苯甲酸甲酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
Wilson, Daniela A.; Wilson, Christopher J.; Rosen, Brad M.; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 21 p. 4879 - 4882
338396-06-8
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
161497-18-3
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 4 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
1: potassium phosphate / tetrahydrofuran 2: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine / tetrahydrofuran / 1.7 h / 20 °C / Inert atmosphere View Scheme
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
338396-06-8
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
1126-46-1
对氯苯甲酸甲酯
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 4 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
619-42-1
对溴苯甲酸甲酯
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 3 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
619-44-3
4-碘苯甲酸甲酯
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 1.7 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
5720-07-0
4-甲氧基苯硼酸
+
161497-18-3
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in water; tert-butyl alcohol T=40°C; Suzuki-Miyaura cross-coupling; 2 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
161497-18-3
+
171364-79-7
4-甲氧基苯硼酸频那醇酯
+
213596-33-9
→
反应条件
729-17-9
4’-甲氧基[1,1’-联苯]-4-甲酸甲酯
反应条件
potassium phosphate; [NiCl(1-naph)(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 3 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
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