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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
213596-33-9
合成路线
（共 94 条）
696-62-8
4-碘苯甲醚
+
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Patent: WO2009/137322 A2, 2009 ;
Location in patent: Page/Page column 21; 22 29; 30; 31 ;
3899-91-0
+
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
potassium phosphate; Ni(COD)2; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA
Patent: WO2009/137322 A2, 2009 ;
Location in patent: Page/Page column 21; 29 ;
1138-62-1
+
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
19013-30-0
4-甲氧基苯基甲磺酸
+
5720-07-0
4-甲氧基苯硼酸
+
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
213596-33-9
→
反应条件
2132-80-1
4,4-二甲氧基联苯
反应条件
1: potassium phosphate / tetrahydrofuran 2: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
→
反应条件
19617-68-6
4-甲氧基-[1,1-联苯]-3-羧酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
161912-35-2
+
213596-33-9
→
反应条件
19617-68-6
4-甲氧基-[1,1-联苯]-3-羧酸甲酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 4 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
1077-02-7
+
213596-33-9
→
反应条件
17171-17-4
4-甲氧基-3-甲基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
40237-72-7
+
213596-33-9
→
反应条件
18648-74-3
反应条件
bis(1,5-cyclooctadiene)nickel (0); cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=20 - 120°C; Inert atmosphere;
参考文献
Shimasaki, Toshiaki; Konno, Yuko; Tobisu, Mamoru; Chatani, Naoto
Organic Letters, 2009 , vol. 11, # 21 p. 4890 - 4892
213596-33-9
→
反应条件
1516-21-8
4-亚硝基苯甲醚
反应条件
NOBF4 in acetonitrile T=20°C; 0.00833333 h;
参考文献
Molander, Gary A.; Cavalcanti, Livia N.
Journal of Organic Chemistry, 2012 , vol. 77, # 9 p. 4402 - 4413
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