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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
213596-33-9
合成路线
（共 94 条）
1137-57-1
+
213596-33-9
→
反应条件
49602-47-3
2,4-二甲氧基联苯
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=20°C; Suzuki-Miyaura cross-coupling; 12 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
98910-57-7
+
213596-33-9
→
反应条件
49602-47-3
2,4-二甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 8 h; Inert atmosphere;
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
213596-33-9
→
反应条件
49602-47-3
2,4-二甲氧基联苯
反应条件
1: potassium phosphate / tetrahydrofuran 2: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; tri-cyclo-hexyl-phosphine / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere View Scheme
参考文献
Zhang, Na; Hoffman, David J.; Gutsche, Nicholas; Gupta, Jayesh; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5956 - 5964
93-04-9
2-萘甲醚
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
bis(1,5-cyclooctadiene)nickel (0); cesium fluoride; tri-cyclo-hexyl-phosphine in toluene T=120°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Tobisu, Mamoru; Shimasaki, Toshiaki; Chatani, Naoto
Angewandte Chemie - International Edition, 2008 , vol. 47, # 26 p. 4866 - 4869
613-46-7
2-萘甲腈
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
CuF2; Ni(PCy3)2Cl2; potassium tert-butylate; tri-cyclo-hexyl-phosphine in 1,4-dioxane T=110°C; Suzuki-Miyaura coupling; 20 h; Inert atmosphere;
参考文献
Yu, Da-Gang; Yu, Miao; Guan, Bing-Tao; Li, Bi-Jie; Zheng, Yang; Wu, Zhen-Hua; Shi, Zhang-Jie
Organic Letters, 2009 , vol. 11, # 15 p. 3374 - 3377
1145-08-0
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
10290-91-2
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
1503-86-2
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 48 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
61912-14-9
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
potassium phosphate; Ni(PCy3)2Cl2 in toluene T=110°C; 24 h;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
115311-03-0
+
213596-33-9
→
反应条件
59115-45-6
(6CI,7CI)-p-2-萘苯甲醚
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in toluene T=120°C; 36 h;
参考文献
Leowanawat, Pawaret; Zhang, Na; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 2 p. 1018 - 1025
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