2-三苯基膦乙烯基丙酸乙酯合成路线 （共 81 条）
反应条件
(i) benzene, (ii) (electrolysis); Multistep reaction;
参考文献
Bestmann,H.J. et al.
Chemische Berichte, 1970 , vol. 103, p. 2794 - 2801
反应条件
(Camphorylsulfonyl)oxaziridine (4) in chloroform T=25°C; 0.5 h;
参考文献
Davis, Franklin A.; Chen, Bang-chi
Journal of Organic Chemistry, 1990 , vol. 55, # 1 p. 360 - 363
反应条件
(Camphorylsulfonyl)oxaziridine (4) in chloroform T=25°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 55, # 1 p. 360 - 363
反应条件
in dichloromethane T=25°C;
参考文献
Kunzmann, Martin H.; Bach, Nina C.; Bauer, Bianca; Sieber, Stephan A.
Chemical Science, 2014 , vol. 5, # 3 p. 1158 - 1167
反应条件
1: dichloromethane / 25 °C 2: N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile / tetrachloromethane / |Reflux View Scheme
参考文献
Chemical Science, , vol. 5, # 3 p. 1158 - 1167
反应条件
T=50°C; P=6750540 Torr; 48 h;
参考文献
Isaacs, Neil S.; El-Din, Ghazi Najim
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2191 - 2192
反应条件
1: tetrahydrofuran / 24 h / Reflux 2: hydrogen / palladium 10 on activated carbon / ethanol / 20 °C View Scheme
参考文献
Metabolex, Inc.
Patent: US2011/313003 A1, 2011 ;
US 20110313003 A1
反应条件
1: tetrahydrofuran / 24 h / Reflux 2: hydrogen / palladium 10 on activated carbon / ethanol / 20 °C View Scheme
参考文献
METABOLEX, INC.; SHI, Dong Fang; SONG, Jiangao; MA, Jingyuan; NOVACK, Aaron; PHAM, Phuongly; NASHASHIBI, Imad; RABBAT, Christopher J.; CHEN, Xin
Patent: WO2011/159297 A1, 2011 ;
WO 2011/159297 A1
反应条件
in dichloromethane T=50°C; 28 h;
参考文献
Volkonskii, A. Yu.; Mysov, E. I.; Rokhlin, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 6 p. 1246 - 1257
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 6 p. 1356 - 1367
反应条件
in dichloromethane T=50°C; 8 h;
参考文献
Volkonskii, A. Yu.; Mysov, E. I.; Rokhlin, E. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, # 6 p. 1246 - 1257
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 6 p. 1356 - 1367
