2-三苯基膦乙烯基丙酸乙酯合成路线 (共 81 条)
反应条件
in dichloromethane
T=20°C; 18 h;
参考文献
D'Ippolito, Giuliana; Iadicicco, Olimpia; Romano, Giovanna; Fontana, Angelo
Tetrahedron Letters, 2002 , vol. 43, # 35 p. 6137 - 6140
反应条件
in chloroform-d1
T=20°C; Isomerization; condensation; dehydration; 62 h;
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
in benzene
2 h; Ambient temperature;
参考文献
Turner,A.D.; Pizzo,S.V.; Rozakis,G.
Journal of the American Chemical Society, 1988 , vol. 110, p. 244
参考文献
Mali, R. S.; Yeola, Suresh N.; Kulkarni, B. K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 4 p. 352 - 354
反应条件
T=50°C; P=6750540 Torr; 48 h;
参考文献
Isaacs, Neil S.; El-Din, Ghazi Najim
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2191 - 2192
反应条件
in dichloromethane
T=20°C; Wittig olefination; 1 h;
参考文献
Yadav; Pratap; Rajender
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5882 - 5885
反应条件
(i), (ii) (electrochemical reduction); Multistep reaction;
参考文献
Nickel; Zimmermann; Preissinger; Fink
Arzneimittel-Forschung/Drug Research, 1978 , vol. 28, # 5 p. 723 - 731
反应条件
in dichloromethane
T=0 - 23°C; Wittig Olefination; 4.08333 h; Inert atmosphere;
参考文献
Xiao, Qing; Young, Kyle; Zakarian, Armen
Organic Letters, 2013 , vol. 15, # 13 p. 3314 - 3317
反应条件
in benzene
T=70°C; Wittig reaction; Title compound not separated from byproducts;
参考文献
Kapferer, Tobias; Brueckner, Reinhard
European Journal of Organic Chemistry, 2006 , # 9 p. 2119 - 2133
反应条件
in toluene
T=60°C; Wittig reaction;
参考文献
Gagey, Nathalie; Neveu, Pierre; Benbrahim, Chouaha; Goetz, Bernard; Aujard, Isabelle; Baudin, Jean-Bernard; Jullien, Ludovic
Journal of the American Chemical Society, 2007 , vol. 129, # 32 p. 9986 - 9998