pyridinium chlorochromate; 4 A molecular sieve in dichloromethane T=20°C; Oxidation; 24 h;
参考文献
Lee, Jeewoo; Kang, Ji-Hye; Lee, Sang-Yoon; Han, Kee-Chung; Torres, Christina M.; Bhattacharyya, Dipak K.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 20 p. 4129 - 4139
1.1: NaH / dimethylformamide / 0.5 h / 20 °C 1.2: 90 percent / dimethylformamide / 4 h / 80 °C 2.1: 92 percent / pyridinium chloroformate; 4A molecular sieve / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Lee, Jeewoo; Kang, Ji-Hye; Lee, Sang-Yoon; Han, Kee-Chung; Torres, Christina M.; Bhattacharyya, Dipak K.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 20 p. 4129 - 4139
1.1: NaH / dimethylformamide / 0.5 h / 20 °C 1.2: 90 percent / dimethylformamide / 4 h / 80 °C 2.1: 92 percent / pyridinium chloroformate; 4A molecular sieve / CH2Cl2 / 24 h / 20 °C View Scheme
参考文献
Lee, Jeewoo; Kang, Ji-Hye; Lee, Sang-Yoon; Han, Kee-Chung; Torres, Christina M.; Bhattacharyya, Dipak K.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 1999 , vol. 42, # 20 p. 4129 - 4139
1: With sodium hydride Heating; 2: With 4 A molecular sieve; pyridinium chlorochromate in dichloromethane Further stages.;
参考文献
Choi, Yongseok; Pu, Yongmei; Peach, Megan L.; Kang, Ji-Hye; Lewin, Nancy E.; Sigano, Dina M.; Garfield, Susan H.; Blumberg, Peter M.; Marquez, Victor E.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 15 p. 3465 - 3481
