(2-甲基-1-氮丙啶基)(苯基)甲酮合成路线 （共 28 条）
反应条件
bis(tricyclohexylphosphane)palladium in toluene
T=70°C; 7 h;
参考文献
Wolfe, John P.; Ney, Joshua E.
Organic Letters, 2003 , vol. 5, # 24 p. 4607 - 4610
反应条件
1.1: diisopropylamine; n-BuLi / tetrahydrofuran; hexane / 0.17 h / 0 °C
1.2: 77 percent / tetrahydrofuran; hexane / 3 h / 0 °C
2.1: 86 percent / potassium hydroxide / ethanol / 0.5 h / 20 °C
3.1: 92 percent / TFA / various solvent(s) / 2 h / 0 °C
View Scheme
参考文献
Schmidt, Dietmar; Conrad, Juergen; Klaiber, Iris; Beifuss, Uwe
Chemical Communications, 2006 , # 45 p. 4732 - 4734
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
2 h; Heating;
参考文献
Werry, Juergen; Stamm, Helmut; Lin, Pen-Yuan; Falkenstein, Reinhard; Gries, Stefan; Irngartinger, Hermann
Tetrahedron, 1989 , vol. 45, # 16 p. 5015 - 5028
反应条件
sodium in tetrahydrofuran
168 h; Further byproducts given;
参考文献
Lin, Pen-Yuan; Bellos, Konstantinos; Werry, Juergen; Assithianakis, Petros; Weiss, Rainer; Mall, Thomas; Bentz, Gunther; Stamm, Helmut
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 3 p. 270 - 278
反应条件
sodium in tetrahydrofuran
168 h; Yield given. Further byproducts given;
参考文献
Lin, Pen-Yuan; Bellos, Konstantinos; Werry, Juergen; Assithianakis, Petros; Weiss, Rainer; Mall, Thomas; Bentz, Gunther; Stamm, Helmut
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 3 p. 270 - 278
反应条件
sodium in tetrahydrofuran
168 h; Yield given. Further byproducts given;
参考文献
Lin, Pen-Yuan; Bellos, Konstantinos; Werry, Juergen; Assithianakis, Petros; Weiss, Rainer; Mall, Thomas; Bentz, Gunther; Stamm, Helmut
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 3 p. 270 - 278
反应条件
lithium anthracene hydride in tetrahydrofuran; hexane
Yield givenFurther byproducts given. Yields of byproduct given;
参考文献
Lin; Stamm
Journal of Chemical Research - Part S, 1998 , # 10 p. 646 - 647
反应条件
n-butyllithium
1.) THF, hexane, 2.) THF, hexane; Yield givenMultistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lin; Stamm
Journal of Chemical Research - Part S, 1998 , # 10 p. 646 - 647
