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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
21388-77-2
合成路线
（共 12 条）
104-21-2
4-甲氧基苄基乙酸酯
+
108-95-2
苯酚
→
反应条件
21388-77-2
反应条件
proton-exchanged montmorillonite in dichloromethane T=20°C;
参考文献
Chen, Dongyin; Xu, Chang; Deng, Jie; Jiang, Chunhuan; Wen, Xiaoan; Kong, Lingyi; Zhang, Ji; Sun, Hongbin
Tetrahedron, 2014 , vol. 70, # 11 p. 1975 - 1983
19962-28-8
1-甲氧基-4-(苯氧基甲基)苯
→
反应条件
21388-77-2
反应条件
cerium trifluoromethanesulfonate in nitromethane T=60°C; 0.5 h;
参考文献
Bartoli, Giuseppe; Dalpozzo, Renato; De Nino, Antonio; Maiuolo, Loredana; Nardi, Monica; Procopio, Antonio; Tagarelli, Antonio
European Journal of Organic Chemistry, 2004 , # 10 p. 2176 - 2180
936007-02-2
→
反应条件
21388-77-2
反应条件
hydrogen; palladium on activated charcoal T=20°C; 1 h;
参考文献
Panda, Gautam; Parai, Maloy Kumar; Das, Sajal Kumar; Shagufta; Sinha, Manish; Chaturvedi, Vinita; Srivastava, Anil K.; Manju; Gaikwad, Anil N.; Sinha, Sudhir
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 3 p. 410 - 419
105-13-5
茴香醇
+
108-95-2
苯酚
→
反应条件
21388-77-2
反应条件
1: (4-methoxyphenyl)methanol With titanium tetrachloride in chloroform T=20°C; 0.0166667 h; Molecular sieve; 2: phenol in chloroform 24 h; Reflux;
参考文献
Tsai, Chen-Yu; Sung, Robert; Zhuang, Bo-Ren; Sung, Kuangsen
Tetrahedron, 2010 , vol. 66, # 34 p. 6869 - 6872
39720-27-9
4-(氯甲基)苯基乙酸酯
+
103594-89-4
→
反应条件
21388-77-2
反应条件
palladium diacetate; tris(4-methylphenyl)-phosphine in toluene T=20°C; 2 h; Inert atmosphere;
参考文献
Chen, Chi-Ren; Zhou, Shuangliu; Biradar, Deepak Baburao; Gau, Han-Mou
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 10 p. 1718 - 1727
61002-54-8
→
反应条件
21388-77-2
反应条件
potassium hydroxide; hydrazine hydrate in diethylene glycol T=190 - 200°C;
参考文献
Kometani; Shiotani
Journal of Medicinal Chemistry, 1978 , vol. 21, # 11 p. 1105 - 1110
107447-97-2
→
反应条件
21388-77-2
反应条件
trifluoroacetic acid in various solvent(s) T=45°C; 1 h; Yields of byproduct given;
参考文献
Torii; Tanaka; Taniguchi; Kameyama; Sasaoka; Shiroi; Kikuchi; Kawahara; Shimabayashi; Nagao
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3633 - 3637
104-92-7
4-溴苯甲醚
→
反应条件
21388-77-2
反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 °C 1.2: 73.3 percent / tetrahydrofuran 2.1: 95.8 percent / H2 / Pd-C / 1 h / 20 °C View Scheme
参考文献
Panda, Gautam; Parai, Maloy Kumar; Das, Sajal Kumar; Shagufta; Sinha, Manish; Chaturvedi, Vinita; Srivastava, Anil K.; Manju; Gaikwad, Anil N.; Sinha, Sudhir
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 3 p. 410 - 419
4397-53-9
4-苄氧基苯甲醛
→
反应条件
21388-77-2
反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 °C 1.2: 73.3 percent / tetrahydrofuran 2.1: 95.8 percent / H2 / Pd-C / 1 h / 20 °C View Scheme
参考文献
Panda, Gautam; Parai, Maloy Kumar; Das, Sajal Kumar; Shagufta; Sinha, Manish; Chaturvedi, Vinita; Srivastava, Anil K.; Manju; Gaikwad, Anil N.; Sinha, Sudhir
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 3 p. 410 - 419
132182-78-6
+
108-95-2
苯酚
→
反应条件
21388-77-2
反应条件
trifluoroacetic acid T=60°C; 1.2 h; other acid catalysts or no acid, other carboxylic esters; Product distribution;
参考文献
Tanaka, Hideo; Taniguchi, Masatoshi; Kameyama, Yutaka; Torii, Sigeru; Sasaoka, Michio; Shiroi, Takashi; Kikuchi, Ryo; Kawahara, Ichiro; Shimabayashi, Akihiro; Nagao, Sigemitsu
Tetrahedron Letters, 1990 , vol. 31, # 46 p. 6661 - 6662
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