1-氨基-2,3-二氢-1H-茚-1-甲醇合成路线 （共 3 条）
反应条件
hydrogen; nickel in ethanol T=55°C; P=25857.4 Torr; 12 h;
参考文献
Rychnovsky, Scott D.; Beauchamp, Thomas; Vaidyanathan, Rajappa; Kwan, Tricia
Journal of Organic Chemistry, 1998 , vol. 63, # 18 p. 6363 - 6374
反应条件
1: With sodium tetrahydroborate in ethanol; water 4 h; Heating / reflux; 2: With sodium hydroxide in diethyl ether; ethanol; water
参考文献
ABBOTT LABORATORIES
Patent: WO2008/133753 A2, 2008 ;
Location in patent: Page/Page column 134 ;
反应条件
1: 89 percent / NaOMe / tetrahydrofuran; methanol / 3 h / Heating 2: 98 percent / H2 / Raney-Ni / ethanol / 12 h / 55 °C / 25857.4 Torr View Scheme
参考文献
Rychnovsky, Scott D.; Beauchamp, Thomas; Vaidyanathan, Rajappa; Kwan, Tricia
Journal of Organic Chemistry, 1998 , vol. 63, # 18 p. 6363 - 6374
