(1-戊基)三苯基溴化磷合成路线 （共 78 条）
参考文献
Vinczer, Peter; Juvancz, Zoltan; Novak, Lajos; Szantay, Csaba
Acta Chimica Hungarica, 1988 , vol. 125, # 6 p. 797 - 820
反应条件
sodium methylate 1) DMF, 25 deg C, 2 h; 2) DMF, 0 deg C, 4 h.; Yield given. Multistep reaction;
参考文献
Dzhumakulov, T.; Yuldashev, A. M.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 516 - 517
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 538 - 539
反应条件
(i) K, HMPT, (ii) /BRN= 1769551/; Multistep reaction;
参考文献
Bestmann,H.J. et al.
Chemische Berichte, 1971 , vol. 104, p. 65 - 70
反应条件
1: 1.) t-BuOK / 1.) THF, 1 h, 2.) THF, 1 h 2: 98.9 percent / H2 / Wilkenson's catalyst / methanol / 16 h View Scheme
参考文献
Chow; Lai; Holmes; Wijono; Wheeler; Garst
European Journal of Medicinal Chemistry, 1996 , vol. 31, # 3 p. 175 - 186
反应条件
1: 1.) BuLi / 1) THF, hexane, 30 min, room temperature; 2) THF, hexane, room temperature, 3 h 2: 80 percent / 750 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1281 - 1284
反应条件
1: 1.) BuLi / 1) THF, hexane, 30 min, room temperature; 2) THF, hexane, room temperature, 3 h 2: 69 percent / 750 °C View Scheme
参考文献
Aitken, R. Alan; Atherton, J. Ian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 10 p. 1281 - 1284
反应条件
1: NaOEt / tetrahydrofuran / 1 h / 25 °C
2: n-BuLi / toluene / 2 h / 25 °C
3: lithium aluminium hydride / tetrahydrofuran / 4 h / Heating
View Scheme
参考文献
Bestmann; Koschatzky; Vostrowsky
Chemische Berichte, 1979 , vol. 112, # 5 p. 1923 - 1925
反应条件
sodium hydride in tetrahydrofuran; dimethyl sulfoxide
参考文献
Chattopadhyay, A.; Mamdapur, V. R.; Chadha, M. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 2 p. 158 - 159
参考文献
Vinczer, Peter; Juvancz, Zoltan; Novak, Lajos; Szantay, Csaba
Acta Chimica Hungarica, 1988 , vol. 125, # 6 p. 797 - 820
反应条件
sodium methylate
1) DMF, 25 deg C, 2 h; 2) DMF, 0 deg C, 4 h.; Yield given. Multistep reaction;
参考文献
Dzhumakulov, T.; Yuldashev, A. M.; Abduvakhabov, A. A.
Chemistry of Natural Compounds, 1982 , vol. 18, # 4 p. 516 - 517
Khimiya Prirodnykh Soedinenii, 1982 , vol. 18, # 4 p. 538 - 539
