1,8-二甲基-1,4,8,11-四氮杂环十四烷合成路线 (共 4 条)
反应条件
hydrogen; nickel in ethanol; ammonia T=336°C; P=98800 Torr;
参考文献
Helvetica Chimica Acta, , vol. 81, # 10 p. 1765 - 1772
反应条件
1: 90 percent / acetonitrile / 2 h / 20 °C 2: aq. NaOH / 3 h View Scheme
参考文献
European Journal of Organic Chemistry, , # 9 p. 1971 - 1975
反应条件
1: 65 percent / acetonitrile / 72 h 2: H2O; NaOH / 2 h View Scheme
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 65, # 2 p. 243 - 266
反应条件
1: 1,4,8,11-tetraazacyclo-tetradecane With formaldehyd; water 2: methyl iodide in acetonitrile 3: With sodium hydroxide in chloroform
参考文献
Chemistry - A European Journal, , vol. 18, # 6 p. 1700 - 1710