2-叔丁基-异吲哚-1,3-二酮合成路线 (共 27 条)
反应条件
ethanol; hydrazine hydrate
参考文献
Smith; Emerson
Org. Synth. Coll. Vol. III<1955>152
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Smith; Emerson
Journal of the American Chemical Society, 1945 , vol. 67, p. 1862
反应条件
triethylamine in dichloromethane
T=23 - 25°C; Inert atmosphere;
参考文献
Goodman, Cassie A.; Hamaker, Christopher G.; Hitchcock, Shawn R.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 6012 - 6014
反应条件
triethylamine in dichloromethane
T=23 - 25°C; Inert atmosphere;
参考文献
Goodman, Cassie A.; Hamaker, Christopher G.; Hitchcock, Shawn R.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 6012 - 6014
反应条件
palladium diacetate; triethylamine; triphenylphosphine in N,N-dimethyl-formamide
T=50°C; P=760.051 Torr; 72 h;
参考文献
Marosvoelgyi-Hasko, Diana; Petz, Andrea; Takacs, Attila; Kollar, Laszlo
Tetrahedron, 2011 , vol. 67, # 47 p. 9122 - 9128
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium 10 on activated carbon in toluene
T=120°C; P=4654.46 Torr; 2 h; Autoclave;
参考文献
Khedkar, Mayur V.; Khan, Shoeb R.; Sawant, Dinesh N.; Bagal, Dattatraya B.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3415 - 3422
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium 10 on activated carbon in toluene
T=120°C; P=4654.46 Torr; 2 h; Autoclave;
参考文献
Khedkar, Mayur V.; Khan, Shoeb R.; Sawant, Dinesh N.; Bagal, Dattatraya B.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3415 - 3422
反应条件
1,4-diaza-bicyclo[2.2.2]octane; palladium 10 on activated carbon in toluene
T=120°C; P=4654.46 Torr; 2 h; Autoclave;
参考文献
Khedkar, Mayur V.; Khan, Shoeb R.; Sawant, Dinesh N.; Bagal, Dattatraya B.; Bhanage, Bhalchandra M.
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3415 - 3422
反应条件
cesium fluoride in acetonitrile
T=30°C; 24 h; Inert atmosphere;
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
18-crown-6 ether in various solvent(s)
5 h; Irradiation;
参考文献
Russell, Glen A.; Khanna, Rajive K.
Tetrahedron, 1985 , vol. 41, # 19 p. 4133 - 4146
反应条件
[bis(acetoxy)iodo]benzene in neat (no solvent)
T=120°C; 0.333333 h; Microwave irradiationGreen chemistry;
参考文献
Vanjari, Rajeshwer; Kumar Allam, Bharat; Nand Singh, Krishna
RSC Advances, 2013 , vol. 3, # 6 p. 1691 - 1694