(3S)-3-羟基-癸酸乙酯合成路线 (共 3 条)
反应条件
in ethanol T=0°C; transesterification; 20 h; Title compound not separated from byproducts.;
参考文献
Fukuzawa, Shin-Ichi; Matsuzawa, Hiroshi; Yoshimitsu, Shin-Ichi
Journal of Organic Chemistry, 2000 , vol. 65, # 6 p. 1702 - 1706
反应条件
in water T=27°C; 24 h; Geotrichum candidum; Title compound not separated from byproducts;
参考文献
Buisson, Didier; Azerad, Robert; Sanner, Caroline; Larcheveque, Marc
Tetrahedron: Asymmetry, 1991 , vol. 2, # 10 p. 987 - 988
反应条件
samarium diiodide; sodium ethanolate 1.) THF, -78 deg C, 0.5 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Fukuzawa, Shin-Ichi; Tatsuzawa, Masahiro; Hirano, Kohki
Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6899 - 6900