2-(4-甲氧基苯基)异吲哚-1,3-二酮合成路线 (共 46 条)
反应条件
copper
T=240°C; 12 h;
参考文献
Yamamoto, Takakazu; Kurata, Yasundo
Canadian Journal of Chemistry, 1983 , vol. 61, p. 86 - 91
反应条件
1: titanium tetrachloride / chlorobenzene / 3 h / 20 °C / |Reflux
2: air / acetonitrile / 0.33 h / 0 °C / |Irradiation
View Scheme
参考文献
Kawai, Masayuki; Sakanoshita, Eriko; Akita, Motoko; Kobayashi, Keiji
Heterocycles, 2013 , vol. 87, # 6 p. 1289 - 1299
反应条件
palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane
T=110°C; 3 h;
参考文献
Begouin, Agathe; Queiroz, Maria-Joao R. P.
European Journal of Organic Chemistry, 2009 , # 17 p. 2820 - 2827
反应条件
1: toluene-4-sulfonic acid / neat (no solvent, solid phase) / 0.08 h / |Milling; |Green chemistry
2: dicyclohexyl-carbodiimide / neat (no solvent, solid phase) / |Milling; |Green chemistry
View Scheme
参考文献
Kumar, Padam Praveen; Rama Devi; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1166 - 1171
反应条件
air; TNF in pyridine
5 h; Heating;
参考文献
Hassan, Alaa A.; Doepp, Dietrich; Henkel, Gerald
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 1 p. 121 - 128
反应条件
1: dichloromethane / 20 °C / |Inert atmosphere
2: dichloromethane / 20 °C / |Inert atmosphere
View Scheme
参考文献
Goodman, Cassie A.; Hamaker, Christopher G.; Hitchcock, Shawn R.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 6012 - 6014
反应条件
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in N,N-dimethyl-formamide
T=100°C; 0.5 h;
参考文献
Kumar, Padam Praveen; Reddy, Y. Dathu; Kumari, Y. Bharathi; Devi, B. Rama; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2014 , vol. 53, # 4 p. 392 - 398
反应条件
[iridium(III)(2-phenylpyridine)3] in acetonitrile
T=20°C; 24 h; Sealed tubeIrradiation; Overall yield = 81percent; regioselective reaction;
参考文献
Allen, Laura J.; Cabrera, Pablo J.; Lee, Melissa; Sanford, Melanie S.
Journal of the American Chemical Society, 2014 , vol. 136, # 15 p. 5607 - 5610
反应条件
air in pyridine
5 h; Heating;
参考文献
Hassan, Alaa A.; Doepp, Dietrich; Henkel, Gerald
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 1 p. 121 - 128
参考文献
Carloni; Carloni, Patricia; Greci; Greci, Lucedio; Stipa; Stipa, Pierluigi; Dopp; Doepp, Dietrich; El-Din Abdel Hafeez Hassan; Hassan, Alaa El-Din Abdel Hafeez; Alberti; Alberti, Angelo
Tetrahedron, 1995 , vol. 51, # 27 p. 7451 - 7458