3-碘代-4-硝基茴香醚合成路线 （共 11 条）
反应条件
1: With sulfuric acid; sodium nitrite in water T=0°C; 2 h; 2: With potassium iodide in water
参考文献
Zhang, Yong Jian; Wei, Hao; Zhang, Wanbin
Tetrahedron, 2009 , vol. 65, # 7 p. 1281 - 1286
反应条件
potassium hydroxide in dimethyl sulfoxide T=18°C; 4 h;
参考文献
Banwell, Martin G.; Jones, Matthew T.; Loong, David T.J.; Lupton, David W.; Pinkerton, David M.; Ray, Jayanta K.; Willis, Anthony C.
Tetrahedron, 2010 , vol. 66, # 47 p. 9252 - 9262
反应条件
sulfuric acid; nitric acid T=0°C;
参考文献
Synlett, , # 11 p. 1674 - 1678
反应条件
1: alcohol; diluted sulfuric acid; sodium nitrate / 15 °C 2: natrium carbonate View Scheme
参考文献
Journal of the Chemical Society, , p. 634
Journal of the Chemical Society, , vol. 127, p. 1602
反应条件
nitric acid; acetic acid
参考文献
Journal of Medicinal Chemistry, , vol. 53, # 2 p. 699 - 714
参考文献
Journal of the Chemical Society, , p. 634
Journal of the Chemical Society, , vol. 127, p. 1602
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
反应条件
iron; ammonium chloride in methanol; water T=50°C;
参考文献
Xi, Jie; Dong, Qing-Li; Liu, Guan-Sai; Wang, Shaozhong; Chen, Lin; Yao, Zhu-Jun
Synlett, 2010 , # 11 p. 1674 - 1678
反应条件
sodium carbonate; Pd2(PPh3)2Cl2 in 1,4-dioxane; water
Suzuki cross-coupling; 12 h; Heating;
参考文献
Kearney, Aaron M.; Vanderwal, Christopher D.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 46 p. 7803 - 7806
