4-甲基-4'-硝基联苯合成路线 (共 71 条)
反应条件
C22H25ClNPPdS; potassium carbonate in 1,4-dioxane
T=100°C; 16 h; Inert atmosphereSchlenk technique;
参考文献
Paluru, Dilip K.; Dey, Sandip; Chaudhari, Kamal R.; Khedkar, Mayur V.; Bhanage, Bhalachandra M.; Jain, Vimal K.
Tetrahedron Letters, 2014 , vol. 55, # 18 p. 2953 - 2956
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
palladium diacetate; SIDip*HCl in 1,4-dioxane
T=100°C; P=760 Torr; 5 h;
参考文献
Andrus, Merritt B.; Ma, Yudao; Zang, Yunfu; Song, Chun
Tetrahedron Letters, 2002 , vol. 43, # 50 p. 9137 - 9140
反应条件
potassium phosphate; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Banerjee, Debasis; Jadhav, Deepak N.
Tetrahedron Letters, 2007 , vol. 48, # 38 p. 6644 - 6647
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide
T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide
T=90°C; 2 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
potassium fluoride in dimethyl sulfoxide
T=105°C; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Huang, Dan-Feng
European Journal of Organic Chemistry, 2010 , # 3 p. 416 - 419
反应条件
sodium carbonate; polystyrene-supported N-heterocyclic carbene-Pd complex in tetrahydrofuran
Suzuki cross-coupling; 13 h; Heating;
参考文献
Zhang, Sujuan; Zeng, Xiaoming; Wei, Zhijun; Zhao, Dongbing; Kang, Tairan; Zhang, Weifeng; Yan, Mei; Luo, Meiming
Synlett, 2006 , # 12 p. 1891 - 1894
反应条件
tetra-(n-butyl)ammonium iodide; (Ph3P)2Pd(Ph)(I) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 1 h;
参考文献
Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 10 p. 1993
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 10 p. 2413 - 2414
反应条件
palladium diacetate in ethanol
T=95°C; 0.25 h; microwave irradiation;
参考文献
Kabalka, George W.; Zhou, Li-Li; Naravane, Abhijit
Tetrahedron Letters, 2006 , vol. 47, # 38 p. 6887 - 6889