4-甲基-4'-硝基联苯合成路线 (共 71 条)
反应条件
tetrabutyl ammonium fluoride; tris-(o-tolyl)phosphine; dichloro bis(acetonitrile) palladium(II)
T=80°C; Hiyama cross-coupling reaction; 1 h;
参考文献
Li, Jin-Heng; Deng, Chen-Liang; Xie, Ye-Xiang
Synthesis, 2006 , # 6 p. 969 - 974
反应条件
water; palladium diacetate; sodium carbonate
T=80°C; Suzuki Coupling; 1 h; Green chemistry;
参考文献
Liu, Leifang; Dong, Yan; Tang, Nana
Green Chemistry, 2014 , vol. 16, # 4 p. 2185 - 2189
反应条件
bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide
T=80°C; Stille carbonylative cross-coupling; P=760.051 Torr; 6 h;
参考文献
Cai, Mingzhong; Zheng, Guomin; Ding, Guodong
Green Chemistry, 2009 , vol. 11, # 10 p. 1687 - 1693
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane
T=20°C; Suzuki-Miyaura coupling; 8 h; Inert atmosphere;
参考文献
Nan, Guangming; Ren, Fang; Luo, Meiming
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 70
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
sodium carbonate; palladium dichloride in methanol
T=20°C; Suzuki-Miyaura cross-coupling reaction; 3 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
aluminium hydroxide-supported palladium nanoparticles in methanol
T=20°C; Suzuki-Miyaura cross-coupling; 4 h; chemoselective reaction;
参考文献
Li, Xing; Yan, Xu-Ying; Chang, Hong-Hong; Wang, Li-Chao; Zhang, Yan; Chen, Wen-Wen; Li, Yan-Wei; Wei, Wen-Long
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 495 - 497
反应条件
aluminium hydroxide-supported palladium nanoparticles in methanol
T=0°C; Suzuki-Miyaura cross-coupling; 12 h;
参考文献
Li, Xing; Yan, Xu-Ying; Chang, Hong-Hong; Wang, Li-Chao; Zhang, Yan; Chen, Wen-Wen; Li, Yan-Wei; Wei, Wen-Long
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 495 - 497
反应条件
palladium 10 on activated carbon; tetrabutyl ammonium fluoride; water; tris(p-fluoro phenyl)phosphine in toluene
T=120°C; Hiyama coupling; 12 h; Inert atmosphere;
参考文献
Monguchi, Yasunari; Yanase, Takayoshi; Mori, Shigeki; Sajiki, Hironao
Synthesis (Germany), 2013 , vol. 45, # 1 art. no. SS-2012-Z0714-PSP, p. 40 - 44
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide
T=20°C; 3 h;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Beletskaya, I. P.
Doklady Chemistry, 1984 , vol. 274, p. 39 - 42
Doklady Akademii Nauk SSSR, 1984 , vol. 274, # 4 p. 818 - 822