4-甲氧基-4'-硝基联苯合成路线 （共 81 条）
反应条件
C12H10N3OPol; tetrabutylammomium bromide; palladium diacetate; potassium carbonate in water T=100°C; Suzuki-Miyaura reaction; 15 h;
参考文献
Adidou, Ouissam; Goux-Henry, Catherine; Safi, Mohamed; Soufiaoui, Mohamed; Framery, Eric
Tetrahedron Letters, 2008 , vol. 49, # 50 p. 7217 - 7219
反应条件
palladium diacetate; 4-Ph2P-C6H4-2-N-glucosamine; sodium carbonate in tetrahydrofuran; ethanol; water T=60°C; 18 h;
参考文献
Kolodziuk, Robert; Penciu, Alexandra; Tollabi, Mustapha; Framery, Eric; Goux-Henry, Catherine; Iourtchenko, Alexander; Sinou, Denis
Journal of Organometallic Chemistry, 2003 , vol. 687, # 2 p. 384 - 391
反应条件
copper(l) iodide; tri-tert-butyl phosphine; cesium fluoride; palladium dichloride in N,N-dimethyl-formamide T=45°C; Stille reaction; 15 h;
参考文献
Mee, Simon P. H.; Lee, Victor; Baldwin, Jack E.
Chemistry - A European Journal, 2005 , vol. 11, # 11 p. 3294 - 3308
反应条件
1: 4-nitro-aniline With tert.-butylnitrite; boron trifluoride diethyl etherate in methanol T=0°C; 0.5 h; Schlenk technique; 2: (4-methoxyphenyl)-boronic acid in methanol T=0 - 60°C; 5 h; Schlenk technique;
参考文献
Zong, Yan; Hu, Jiefeng; Sun, Peipei; Jiang, Xiaoqing
Synlett, 2012 , vol. 23, # 16 art. no. ST-2012-W0506-L, p. 2393 - 2396
反应条件
NHC-Pd(II)-Im; tetrabutyl ammonium fluoride in toluene T=120°C; Hiyama reaction; 3 h; Inert atmosphere;
参考文献
Gu, Zheng-Song; Shao, Li-Xiong; Lu, Jian-Mei
Journal of Organometallic Chemistry, 2012 , vol. 700, p. 132 - 134
反应条件
sodium carbonate; tris[(perfluoroalkyl)phenyl]phosphane palladium in methanol T=75°C; Suzuki coupling; 2 h;
参考文献
Scheuermann, Gil M.; Steurer, Peter; Muelhaupt, Rolf; Rumi, Luigi; Bannwarth, Willi
Journal of the American Chemical Society, 2009 , vol. 131, # 23 p. 8262 - 8270
反应条件
5 Pd/BaCO3 in methanol T=25°C; 12 h;
参考文献
Felpin, Francois-Xavier; Fouquet, Eric
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 6 p. 863 - 868
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium lauryl sulfate; potassium carbonate; p-toluenesulfonyl chloride in water T=60°C; Suzuki Coupling;
参考文献
Liu, Jin-Biao; Zhou, He-Ping; Peng, Yi-Yuan
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2872 - 2875
反应条件
KF in tetrahydrofuran
参考文献
Yale University
Patent: US6562989 B2, 2003 ;
反应条件
tetrakis(triphenylphosphine) palladium(0); silver(l) oxide in tetrahydrofuran T=60°C; Arylation; 36 h;
参考文献
Hirabayashi, Kazunori; Kawashima, Jun; Nishihara, Yasushi; Mori, Atsunori; Hiyama, Tamejiro
Organic Letters, 1999 , vol. 1, # 2 p. 299 - 301
