4-甲氧基-4'-硝基联苯合成路线 （共 81 条）
反应条件
diphenylphosphine-based palladium(0) complex on MCM-41 in water; N,N-dimethyl-formamide T=60°C; Stille coupling; 6 h;
参考文献
Zhao, Hong; Wang, Yue; Sha, Junchao; Sheng, Shouri; Cai, Mingzhong
Tetrahedron, 2008 , vol. 64, # 32 p. 7517 - 7523
反应条件
sodium 2-(2-pyridin-3-ylethylamino)ethyl sulfonate; palladium dichloride in water T=20°C; Suzuki coupling; 3 h;
参考文献
Pawar, Shivaji S.; Uppalla, Lavkumar S.; Shingare, Murlidhar S.; Thore, Shivaji N.
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5858 - 5862
反应条件
[(P{(NC5H10)(C6H11)2})2Pd(Cl)2] in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=100°C; Negishi cross-coupling reaction; 0.0833333 h; In air;
参考文献
Bolliger, Jeanne L.; Frech, Christian M.
Chemistry - A European Journal, 2010 , vol. 16, # 36 p. 11072 - 11081
反应条件
sodium carbonate; palladium dichloride in methanol T=20°C; Suzuki-Miyaura cross-coupling reaction; 0.333333 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
sodium carbonate; palladium dichloride in methanol T=20°C; Suzuki-Miyaura cross-coupling reaction; 3 h;
参考文献
Zhou, Wen-Jun; Wang, Ke-Hu; Wang, Jin-Xian; Gao, Zhi-Rong
Tetrahedron, 2010 , vol. 66, # 38 p. 7633 - 7641
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 12 h;
参考文献
Amatore, Christian; Jutand, Anny; Negri, Serge; Fauvarque, Jean-Francois
Journal of Organometallic Chemistry, 1990 , vol. 390, # 3 p. 389 - 398
反应条件
1: p-anisylgermanium trichloride With ammonium hydroxide T=20°C; 1 h; 2: para-nitro iodo-benzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water 4 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
1: p-anisylgermanium trichloride With ammonium hydroxide T=20°C; 2: 1-bromo-4-nitro-benzene With sodium hydroxide; palladium diacetate in 1,4-dioxane; water 8 h; Heating; Further stages.;
参考文献
Advanced Synthesis and Catalysis, , vol. 349, # 7 p. 1025 - 1027
反应条件
1.1: BuLi / diethyl ether; hexane / 1 h / -78 °C 1.2: 63 percent / diethyl ether; hexane / 13 h / 20 °C 2.1: 45 percent / Ag2O / Pd(PPh3)4 / tetrahydrofuran / 36 h / 60 °C View Scheme
参考文献
Organic Letters, , vol. 1, # 2 p. 299 - 301
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; potassium carbonate in dimethyl sulfoxide T=110°C; Hiyama coupling;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
