4-[[(4-二甲基氨基苯基)甲亚基肼亚基]甲基]-N,N-二甲基苯胺合成路线 (共 20 条)
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide
T=20°C; 24 h; Title compound not separated from byproducts;
参考文献
Nenajdenko, Valentine G.; Varseev, Georgy N.; Shastin, Alexey V.; Balenkova, Elisabeth S.
Journal of Fluorine Chemistry, 2005 , vol. 126, # 6 p. 907 - 913
反应条件
1: silica gel / dichloromethane / Microwave irradiation
2: silica gel / dichloromethane / Microwave irradiation
View Scheme
参考文献
Chattopadhyay, Gautam; Ray, Partha Sinha
Synthetic Communications, 2011 , vol. 41, # 17 p. 2607 - 2614
反应条件
hydrazine hydrate in ethanol
参考文献
O'Callaghan,C.N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 1416 - 1419
反应条件
hydrazine in ethanol; benzene
参考文献
Pohloudek-Fabini,R.; Froehling,D.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1965 , vol. 298, p. 423 - 434
反应条件
silica gel in dichloromethane
Microwave irradiation;
参考文献
Chattopadhyay, Gautam; Ray, Partha Sinha
Synthetic Communications, 2011 , vol. 41, # 17 p. 2607 - 2614
反应条件
silica gel in dichloromethane
Microwave irradiation;
参考文献
Chattopadhyay, Gautam; Ray, Partha Sinha
Synthetic Communications, 2011 , vol. 41, # 17 p. 2607 - 2614
参考文献
Hiller,S.A. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1970 , vol. 6, p. 430 - 435
Khimiya Geterotsiklicheskikh Soedinenii, 1970 , vol. 6, p. 466 - 471
参考文献
Knoepfer
Monatshefte fuer Chemie, 1909 , vol. 30, p. 33
参考文献
Curtius; Bertho
Journal fuer Praktische Chemie (Leipzig), 1930 , vol. <2> 125, p. 23,39
反应条件
in 1,2-dichloro-ethane
96 h; Ambient temperature;
参考文献
Saito, Takao; Oikawa, Isao; Motoki, Shinichi
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 4 p. 1023 - 1027