(1S,2S)-(+)-1,2-环己二胺合成路线 （共 35 条）
反应条件
hydrogen; palladium dihydroxide in methanol T=20°C; P=2068.59 Torr; 48 h;
参考文献
Chandrasekhar; Sekar; Singh
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 10079 - 10083
反应条件
Candida antarctica lipase on acrylic resin in 1,4-dioxane T=20°C;
参考文献
Tumambac, Gilbert E.; Wolf, Christian
Organic Letters, 2005 , vol. 7, # 18 p. 4045 - 4048
反应条件
1: With L-(+)-tartaric acid; acetic acid in methanol; water 24 h; Heating; 2: With hydrogenchloride in acetone 25 h; Heating; 3: With sodium hydroxide
参考文献
Tetrahedron Asymmetry, , vol. 14, # 18 p. 2763 - 2769
反应条件
(2S,3S)-2,3-dihydroxybutanedioic acid Resolution of racemate;
参考文献
Canta, Merce; Font, David; Gomez, Laura; Ribas, Xavi; Costas, Miquel
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 818 - 830
反应条件
in water; acetic acid
反应条件
1: 95 percent / LiClO4 / acetonitrile / 48 h / 20 °C 2: 75 percent / diisopropyl azodicarboxylate; Ph3P / CH2Cl2 / 7 h / 0 - 20 °C 3: TMSN3 / acetonitrile / 7 h / 20 °C 4: 95 percent / H2 / Pd(OH)2/C / methanol / 48 h / 20 °C / 2068.59 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 51 p. 10079 - 10083
反应条件
1: TMSN3 / acetonitrile / 7 h / 20 °C 2: 95 percent / H2 / Pd(OH)2/C / methanol / 48 h / 20 °C / 2068.59 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 51 p. 10079 - 10083
反应条件
1: 75 percent / diisopropyl azodicarboxylate; Ph3P / CH2Cl2 / 7 h / 0 - 20 °C 2: TMSN3 / acetonitrile / 7 h / 20 °C 3: 95 percent / H2 / Pd(OH)2/C / methanol / 48 h / 20 °C / 2068.59 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 51 p. 10079 - 10083
反应条件
immobilised Candida antarctica lipase (NOVOZYM 435) in 1,4-dioxane 9 h;
参考文献
Chemical Communications, , # 21 p. 2471 - 2472
反应条件
immobilised Candida antarctica lipase (NOVOZYM 435) in 1,4-dioxane 7 h;
参考文献
Chemical Communications, , # 21 p. 2471 - 2472
