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hydrogenchloride in dichloromethane; pentane addn. of HCl gas to a soln. of Re-compd. in CH2Cl2 and pentane at -78°C, kept at -78°C for 20 min, warmed to 25°C over 45 min; addn. of CH2Cl2, filtered through Celite, concd., cooled, crystn. from a mixture of CH2Cl2 and pentane; elem. anal.;

hydrogenchloride in water

in dichloromethane; toluene ReO3(OSiMe3) and isocyanate in toluene refluxed for 24 h, removal of solvent in vac., redissolved in CH2Cl2, addn. of pyridine*HCl, 2 h; addn. of pentane, concn. in vac., filtered through Celite, reduced to dryness in vac., extn. (boiling benzene), filtered (ArNH3Cl and Py*HCl), concn. of filtrate, cooled, recrystn. (CH2Cl2/pentane); elem. anal.;

hydrogenchloride; tin(ll) chloride in ethanol; water T=30°C; Rate constantMechanism;

sodium hydroxide; phosphorous pentoxide; N,N-dimethyl-cyclohexylamine 1) 170 deg C, 1.5 h; 2) 100 deg C, 1 h; Yield given. Multistep reaction;

in water T=250°C; 24 h;