4-(4,4,5,5-四甲基-1,3,2-二氧杂硼烷-2-基)氟苯合成路线 （共 26 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=60°C; Suzuki-Miyaura coupling; 0.0833333 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 16 p. 4165 - 4171
反应条件
1: With lithium bis((trifluoromethyl)sulfonyl)amide in tetrahydrofuran T=20°C; Electrochemical reaction; 2: With sulfuric acid T=0°C; pH=5; Further stages.;
参考文献
Laza, Carine; Dunach, Elisabet
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 5 p. 580 - 583
反应条件
triphenylphosphine in tetrahydrofuran; water T=-78 - -55°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 133, # 7 p. 2116 - 2119
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium phosphate; palladium diacetate in neat (no solvent)
T=60°C; Suzuki-Miyaura Coupling; 24 h; Schlenk techniqueInert atmosphere;
参考文献
Asachenko, Andrey F.; Sorochkina, Kristina R.; Dzhevakov, Pavel B.; Topchiy, Maxim A.; Nechaev, Mikhail S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3553 - 3557
反应条件
palladium diacetate; triphenylphosphine in 1,4-dioxane
T=100°C; 15 h; Inert atmosphere;
参考文献
Wu, Yusheng; Li, Xinjian; Zou, Dapeng; Zhu, Helong; Wang, Yaping; Li, Jingya; Wu, Yangjie
Organic Letters, 2014 , vol. 16, # 7 p. 1836 - 1839
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide
T=90°C; Suzuki-Miyaura Coupling; 24 h; Schlenk technique;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
