4-乙酰基氨基苯硼酸频哪醇酯合成路线 （共 14 条）
反应条件
tert.-butylnitrite; dibenzoyl peroxide in acetonitrile T=20°C; Sandmeyer reaction; 2 h;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 10 p. 1846 - 1849
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 5 h;
参考文献
US6680401 B1, ;
Page column 19 ;
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; borylation; 4 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
pyridine in tetrahydrofuran T=20°C; 4 h;
参考文献
WO2006/51851 A1, ;
Page/Page column 73 ;
反应条件
in ethanol T=20°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 54, # 2 p. 166 - 169
反应条件
2: 77 percent / Et3N / PdCl2(dppf) / dioxane / 4 h / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 164 - 168
反应条件
1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / ethanol / 2 h / 80 °C / |Inert atmosphere 2: ethanol / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 2 p. 166 - 169
参考文献
Journal of the American Chemical Society, , vol. 127, # 38 p. 13094 - 13095
反应条件
sodium salt of phosphorous acid; palladium on activated charcoal in water; isopropyl alcohol T=20°C; Suzuki-Miyaura cross-coupling; 10 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
反应条件
1.1: sodium hydrogencarbonate / water; ethanol; toluene / 0.25 h / |Inert atmosphere 1.2: 1 h / 120 °C / |Microwave irradiation; |Inert atmosphere 2.1: hydrogenchloride / methanol / 1 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Conole, Daniel; Beck, Thorsten M.; Jay-Smith, Morgan; Tingle, Malcolm D.; Eason, Charles T.; Brimble, Margaret A.; Rennison, David
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 7 p. 2220 - 2235
