4-乙酰基氨基苯硼酸频哪醇酯合成路线 （共 14 条）
反应条件
water in ethanol T=20°C; Kinetics; Reagent/catalyst;
参考文献
Achilli, Cesare; Ciana, Annarita; Fagnoni, Maurizio; Balduini, Cesare; Minetti, Giampaolo
Central European Journal of Chemistry, 2013 , vol. 11, # 2 p. 137 - 139
反应条件
1.1: sodium hydrogencarbonate / water; ethanol; toluene / 0.25 h / |Inert atmosphere 1.2: 1 h / 120 °C / |Microwave irradiation; |Inert atmosphere 2.1: hydrogenchloride / methanol / 1 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Conole, Daniel; Beck, Thorsten M.; Jay-Smith, Morgan; Tingle, Malcolm D.; Eason, Charles T.; Brimble, Margaret A.; Rennison, David
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 7 p. 2220 - 2235
反应条件
1.1: sodium hydrogencarbonate / water; ethanol; toluene / 0.25 h / |Inert atmosphere
1.2: 1 h / 120 °C / |Microwave irradiation; |Inert atmosphere
2.1: ammonium hydroxide; zinc / tetrahydrofuran / 5 h / |Reflux; |Inert atmosphere
3.1: hydrogenchloride / methanol / 1 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Conole, Daniel; Beck, Thorsten M.; Jay-Smith, Morgan; Tingle, Malcolm D.; Eason, Charles T.; Brimble, Margaret A.; Rennison, David
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 7 p. 2220 - 2235
反应条件
1.1: sodium hydrogencarbonate / water; ethanol; toluene / 0.25 h / |Inert atmosphere
1.2: 1 h / 120 °C / |Microwave irradiation; |Inert atmosphere
2.1: hydrogenchloride / methanol / 1 h / |Inert atmosphere; |Reflux
View Scheme
参考文献
Conole, Daniel; Beck, Thorsten M.; Jay-Smith, Morgan; Tingle, Malcolm D.; Eason, Charles T.; Brimble, Margaret A.; Rennison, David
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 7 p. 2220 - 2235
