4-叔丁基苯硼酸频那醇酯合成路线 （共 15 条）
反应条件
1: 1-bromo-4-(1,1-dimethylethyl)benzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=-78°C; Further stages.;
参考文献
Molecular Crystals and Liquid Crystals, , vol. 471, # 1 p. 89 - 98
反应条件
NiCl2(PMe3)2; TMSOCH2CF3; cesium fluoride in tetrahydrofuran T=100°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 13, # 21 p. 5766 - 5769
反应条件
boron trifluoride diethyl etherate in acetonitrile T=0°C; 0.333333 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 17 p. 4560 - 4563
反应条件
magnesium sulfate in tetrahydrofuran T=20°C; 16 h;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 37 p. 9385 - 9388
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane Heating;
参考文献
Synthesis, , # 4 art. no. M05304SS, p. 547 - 550
反应条件
1: 4-tert-Butylphenylmagnesium bromide With boric acid trimethyl ester in tetrahydrofuran T=-78 - 25°C; 2: 2,3-dimethylbutane-2,3-diol With acetic acid in tetrahydrofuran T=20°C; 4 h;
参考文献
European Journal of Organic Chemistry, , # 23 p. 3964 - 3972
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 2 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
反应条件
in dimethyl sulfoxide T=20°C; 0.5 h;
参考文献
Tetrahedron Letters, , vol. 54, # 2 p. 166 - 169
反应条件
potassium acetate in tert-butyl alcohol T=90°C; 17 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 25 p. 6913 - 6917
反应条件
1: 98 percent / pyridine / CH2Cl2 / 0.25 h / 0 °C 2: 86 percent / Et3N / PdCl2(dppf) / dioxane / Heating View Scheme
参考文献
Synthesis, , # 4 art. no. M05304SS, p. 547 - 550
