3,4,5-三甲氧基苯硼酸频那醇酯合成路线 （共 12 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine in 1,4-dioxane
T=80°C; Masuda borylation; 4 h; Inert atmosphere;
参考文献
Merkul, Eugen; Schaefer, Elisabeth; Mueller, Thomas J. J.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 9 p. 3139 - 3141
反应条件
1.1: tetrafluoroboric acid / water / 0.17 h / 0 °C
1.2: 1 h / 0 °C
1.3: 2.5 h / 20 °C / |Inert atmosphere
2.1: diethyl ether / 4 h / 20 °C
View Scheme
参考文献
Marciasini, Ludovic D.; Richy, Nicolas; Vaultier, Michel; Pucheault, Mathieu
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 6 p. 1083 - 1088
