2,4,6-三甲基苯硼酸新戊二醇酯合成路线 （共 9 条）
反应条件
copper(l) iodide; tributyl-amine; potassium tert-butylate in tetrahydrofuran T=20°C;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 5350 - 5354
Angewandte Chemie, , vol. 121, p. 5454 - 5458
反应条件
in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 11 p. 1397 - 1400
反应条件
copper(l) iodide; tributylphosphine; potassium tert-butylate in tetrahydrofuran byproducts: KBr, Me3C6H3; react. of (B(OCH2)2C(CH3)2)2 (1.5 equiv.), 2,4,6-Me3C6H2Br (1 equiv.), CuI (10 molpercent), nBu3P (13 molpercent) and KOtBu (1.5 equiv.) at room temp.; detd. by XRD;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 5350 - 5354
Angewandte Chemie, , vol. 121, p. 5454 - 5458
反应条件
TlOH; tetrakis(triphenylphosphine) palladium(0) in benzene Dehalogenation; Suzuki cross-coupling; Heating;
参考文献
Tetrahedron, , vol. 56, # 49 p. 9655 - 9662
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene Dehalogenation; Suzuki cross-coupling; transesterification; Heating;
参考文献
Tetrahedron, , vol. 56, # 49 p. 9655 - 9662
反应条件
potassium tert-butylate; copper(l) chloride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in tetrahydrofuran T=70°C; P=760.051 Torr; 24 h;
参考文献
Ohishi, Takeshi; Nishiura, Masayoshi; Hou, Zhaomin
Angewandte Chemie - International Edition, 2008 , vol. 47, # 31 p. 5792 - 5795
反应条件
bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate in tetrahydrofuran T=20°C; Chan-Lam type coupling; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645
反应条件
bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate in tetrahydrofuran T=20°C; Chan-Lam type coupling; 4 h; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645
反应条件
barium dihydroxide; tetrakis(triphenylphosphine) palladium(0) in ethylene glycol dimethyl ether; water
Suzuki cross-coupling reaction; 24 h; Heating;
参考文献
Leslie, Wendy; Batsanov, Andrei S.; Howard, Judith A.K.; Williams, J.A. Gareth
Dalton Transactions, 2004 , # 4 p. 623 - 631
