反应条件
1: 96 percent / LiAlH4 / tetrahydrofuran / 1 h / 21 - 29 °C
2: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2. -65 deg C, 4 h, 2.) CH2Cl2, -65 deg C to -10 deg C, overnight
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参考文献
Rotherham, Lloyd W.; Edward Semple
Journal of Organic Chemistry, 1998 , vol. 63, # 19 p. 6667 - 6672
