4-[(叔丁氧基甲酰)甲基]-2-氰基吡啶合成路线 （共 5 条）
反应条件
N,N-dimethylcarbamoyl chloride in dichloromethane T=20°C; Substitution; 48 h;
参考文献
Yang, Qifei; Olmsted, Courtney; Borhan, Babak
Organic Letters, 2002 , vol. 4, # 20 p. 3423 - 3426
反应条件
1: 95 percent / TEA / tetrahydrofuran / 20 °C 2: 80 percent / mCPBA / CH2Cl2 / 12 h / 20 °C 3: 53 percent / (CH3)2NCOCl / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 4, # 20 p. 3423 - 3426
反应条件
1: 80 percent / mCPBA / CH2Cl2 / 12 h / 20 °C 2: 53 percent / (CH3)2NCOCl / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 4, # 20 p. 3423 - 3426
反应条件
1: 95 percent / TEA / tetrahydrofuran / 20 °C 2: 80 percent / mCPBA / CH2Cl2 / 12 h / 20 °C 3: 53 percent / (CH3)2NCOCl / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 4, # 20 p. 3423 - 3426
反应条件
sodium hydroxide in ethanol Hydrolysis; 24 h; Heating;
参考文献
Huang, Xuefei; Borhan, Babak; Rickman, Barry H.; Nakanishi, Koji; Berova, Nina
Chemistry - A European Journal, 2000 , vol. 6, # 2 p. 216 - 224
