2-甲基-1-萘基溴化镁合成路线 （共 19 条）
反应条件
magnesium in diethyl ether 2 h; Heatingultrasonic heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 2044 - 2046
参考文献
Catch; Evans
Journal of the Chemical Society, 1957 , p. 2796,2799
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene 3 h; Heating;
参考文献
Miyano, Sotaro; Okada, Shin-ichi; Suzuki, Toshiyuki; Handa, Shigeru; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 2044 - 2046
反应条件
iron(III) chloride; 1,2-dichloro-ethane in diethyl ether 12 h; Heating;
参考文献
Nagano, Takashi; Hayashi, Tamio
Organic Letters, 2005 , vol. 7, # 3 p. 491 - 493
反应条件
hydrogenchloride in water; toluene
参考文献
Hoechst Aktiengesellschaft
Patent: US5510554 A1, 1996 ;
参考文献
Cagniant; Cagniant
Bulletin de la Societe Chimique de France, 1958 , p. 1448,1457
反应条件
anschliessende Pyrolyse des Reaktionsprodukts;
参考文献
Arbuzov; Gretschkin
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 1697
p. 1733
反应条件
NiCl2((PPh3)P)2 in diethyl ether; benzene 3 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 2044 - 2046
反应条件
1: 87 percent / benzene; diethyl ether / 1.) 2 h, room temperature, 2.) 3 h, reflux 2: N-bromosuccinimide (NBS), benzoyl peroxide (BPO) / CCl4 / 8 h / Heating 3: 1.) AcOK; 2.) 2 N HCl / 1.) AcOH, 8 h, reflux; 2.) reflux, 30 min 4: 97 percent / KMnO4 / acetone; H2O / 1.5 h / Heating 5: 78 percent / KOH / H2O / 2 h / Heating View Scheme
参考文献
Oi; Matsunaga; Hattori; Miyano
Synthesis, 1993 , # 9 p. 895 - 899
反应条件
2: N2H4; alkali View Scheme
参考文献
Cagniant; Cagniant
Bulletin de la Societe Chimique de France, 1958 , p. 1448,1457
