二(五氟苯基硫基)铅(II)合成路线 （共 7 条）
反应条件
phosphorus pentachloride in pentane
T=0°C;
参考文献
Denney, Donald B.; Denney, Dorothy Z.; Liu, Lun-Tsu
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 1 - 8
反应条件
in pentane
byproducts: (C6F5S)3P; addn. of PCl5 to a suspension of the Pb-compd. in pentane at 0°C and allowing the mixt. to warm to room temp.; sepn. of the pptd. Pb-compd. by filtn., concg. of the remainin soln. at reduced pressure, pptn. of the disulfide upon cooling, sepn. by filtn., obtaining the thiophosphite after concg. the filtrate;
参考文献
Denney, Donald B.; Denney, Dorothy Z.; Liu, Lun-Tsu
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 1 - 8
参考文献
Peach,M.E.; Spinney,H.G.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 644 - 648
反应条件
in tetrachloromethane
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.11, page 32 - 49
参考文献
Peach, M. E.; Spinney, H. G.
Canadian Journal of Chemistry, 1971 , vol. 49, p. 644 - 647
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.10, page 27 - 31
参考文献
Peach, M. E.
Intern. J. Sulfur Chem., 1973 , vol. 8, p. 27 - 29
参考文献
Peach, M. E.
Intern. J. Sulfur Chem., 1973 , vol. 8, p. 27 - 29
