1-(烯丙氧基)-2-丙醇合成路线 (共 7 条)
反应条件
Et3N-BH3; lithium perchlorate in diethyl ether T=20°C; 1 h;
参考文献
Heydari, Akbar; Mehrdad, Morteza; Maleki, Aziz; Ahmadi, Nafiseh
Synthesis, 2004 , # 10 p. 1563 - 1565
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide 1) 30 min, rt, 2) reflux, 4 h;
参考文献
Bailey, William F.; Carson, Matthew W.
Journal of Organic Chemistry, 1998 , vol. 63, # 26 p. 9960 - 9967
反应条件
Cp2Ti(PMe3)2; trimethylphosphane in toluene T=-20°C; Yield given. Yields of byproduct given;
参考文献
Kablaoui, Natasha M.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1995 , vol. 117, # 25 p. 6785 - 6786
参考文献
Takeuchi, Hiroshi; Kitajima, Kunio; Yamamoto, Yasuhiro; Mizuno, Kiyokazu
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 2 p. 199 - 203
反应条件
Cp2Ti(PMe3)2; (Ph)2SiH2; trimethylphosphane 1.) toluene, -20 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kablaoui, Natasha M.; Buchwald, Stephen L.
Journal of the American Chemical Society, 1995 , vol. 117, # 25 p. 6785 - 6786
反应条件
tin(ll) chloride; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran; water T=50°C; 45 h;
参考文献
Masuyama, Yoshiro; Marukawa, Masanori
Tetrahedron Letters, 2007 , vol. 48, # 34 p. 5963 - 5965
反应条件
tin(ll) chloride; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran; water
T=50°C; 46 h;
参考文献
Masuyama, Yoshiro; Marukawa, Masanori
Tetrahedron Letters, 2007 , vol. 48, # 34 p. 5963 - 5965