2-氧代-2,3-二氢吲哚-1-羧酸叔丁酯合成路线 （共 5 条）
反应条件
sodium hydrogencarbonate in tetrahydrofuran Heating;
参考文献
Akai, Shuji; Tsujino, Toshiaki; Naka, Tadaatsu; Tanimoto, Kouichi; Kita, Yasuyuki
Tetrahedron Letters, 2001 , vol. 42, # 41 p. 7315 - 7317
反应条件
sodium carbonate in tetrahydrofuran T=70°C; 12 h;
参考文献
Arizpe, Alicia; Sayago, Francisco J.; Jimenez, Ana I.; Ordonez, Mario; Cativiela, Carlos
European Journal of Organic Chemistry, 2011 , # 16 p. 3074 - 3081
反应条件
1: 0.09 g / 12 h / 25 °C 2: 90 percent / P(OEt)3 / [Rh(COD)Cl]2 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Padwa, Albert; Wang, Qiu
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3210 - 3220
反应条件
sodium carbonate in ethylene glycol dimethyl ether; water 0.25 h; Heating;
参考文献
El Kazzouli, Said; Koubachi, Jamal; Berteina-Raboin, Sabine; Mouaddib, Abderrahim; Guillaumet, Gerald
Tetrahedron Letters, 2006 , vol. 47, # 48 p. 8575 - 8577
反应条件
1.1: LiBEt3H / tetrahydrofuran / 0.5 h / -78 °C
1.2: 63 percent / NaH / tetrahydrofuran / 0 - 20 °C
2.1: 100 percent / CF3COOH / CH2Cl2 / 1.5 h / 0 °C
View Scheme
参考文献
Perron, Julien; Joseph, Benoit; Merour, Jean-Yves
European Journal of Organic Chemistry, 2004 , # 22 p. 4606 - 4613
