1,2:3,4-二苯并蒽合成路线 (共 31 条)
反应条件
boron trifluoride dimethyl etherate in dichloromethane T=20°C; 16 h;
参考文献
Chen, Ya-Li; Wong, Man-Shing; Wong, Wai-Yeung; Lee, Albert W.M.
Tetrahedron Letters, 2007 , vol. 48, # 13 p. 2421 - 2425
反应条件
Al(c-C6H11O)3 in cyclohexanol;
参考文献
Watanabe; Snieckus
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1457 - 1460
反应条件
diiron enneacarbonyl in benzene 40 h; Heating;
参考文献
Moursounidis, John; Wege, Dieter
Australian Journal of Chemistry, 1988 , vol. 41, # 2 p. 235 - 249
反应条件
boron trifluoride dimethyl etherate in dichloromethane T=20°C; 16 h;
参考文献
Chen, Ya-Li; Wong, Man-Shing; Wong, Wai-Yeung; Lee, Albert W.M.
Tetrahedron Letters, 2007 , vol. 48, # 13 p. 2421 - 2425
反应条件
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 16 h; Heating;
参考文献
Lee, Hongmee; Harvey, Ronald G.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 749 - 751
反应条件
trichlorophosphate in pyridine 0.166667 h; Heating;
参考文献
Sukumaran, Kutikat B.; Harvey, Ronald G.
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2740 - 2745
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in various solvent(s) 0.5 h; Heating;
参考文献
Fitzgerald, John J.; Drysdale, Neville E.; Olofson, R. A.
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7122 - 7126
反应条件
1: 90 percent / CsF / PdCl2(PPh3)2 / acetonitrile / 8 h / 20 °C 2: 85 percent / BF3*Et2O / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 24 p. 8445 - 8450
反应条件
lithium hydroxide in dichloromethane 48 h; Ambient temperature;
参考文献
Minsky, Abraham; Rabinovitz, Mordecai
Synthesis, 1983 , # 6 p. 497 - 498
反应条件
1: 91 percent / H2 / 10percent Pd/C / methanol / 760 Torr 2: 95 percent / 520 °C / 0.1 Torr 3: 1.) isoamyl nitrite, trichloroacetic acid / 1.) THF, RT, 2 h, 2.) 1,2-dichloroethane, reflux, 30 min 4: 85 percent / diiron enneacarbonyl / benzene / 40 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 41, # 2 p. 235 - 249