1,2:3,4-二苯并蒽合成路线 (共 31 条)
反应条件
1: 55 percent / tetrahydrofuran / 2 h / Ambient temperature 2: 56 percent / POCl3 / pyridine / 0.17 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 13 p. 2740 - 2745
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene 0.166667 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 169 - 171
反应条件
1: 56 percent / chromous chloride / tetrahydrofuran; aq. NH3 / overnight 2: 56 percent / POCl3 / pyridine / 0.17 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 46, # 13 p. 2740 - 2745
反应条件
trifluorormethanesulfonic acid in CH3Cl T=25°C;
参考文献
Tetrahedron Letters, , vol. 50, # 17 p. 1924 - 1927
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene
参考文献
Tetrahedron Letters, , vol. 28, # 38 p. 4363 - 4366
反应条件
1: NBS, dibenzoyl peroxide / CCl4 / 6 h / Heating 2: dimethylformamide / 8 h / Heating 3: 24 percent / aq. LiOH / CH2Cl2 / 48 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 6 p. 497 - 498
反应条件
1: dimethylformamide / 8 h / Heating 2: 24 percent / aq. LiOH / CH2Cl2 / 48 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 6 p. 497 - 498
反应条件
1: 1.) isoamyl nitrite, trichloroacetic acid / 1.) THF, RT, 2 h, 2.) 1,2-dichloroethane, reflux, 30 min 2: 85 percent / diiron enneacarbonyl / benzene / 40 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 41, # 2 p. 235 - 249
反应条件
1: 95 percent / 520 °C / 0.1 Torr 2: 1.) isoamyl nitrite, trichloroacetic acid / 1.) THF, RT, 2 h, 2.) 1,2-dichloroethane, reflux, 30 min 3: 85 percent / diiron enneacarbonyl / benzene / 40 h / Heating View Scheme
参考文献
Australian Journal of Chemistry, , vol. 41, # 2 p. 235 - 249
参考文献
Journal of the American Chemical Society, , vol. 59, p. 2339,2341
Journal of the American Chemical Society, , vol. 56, p. 1363
Journal of the American Chemical Society, , vol. 57, p. 555