3,5-二甲氧基苯甲酸甲酯合成路线 （共 80 条）
反应条件
aluminium trichloride
参考文献
Sassa, Takeshi; Nukina, Manabu; Suzuki, Yoshikatsu
Agricultural and Biological Chemistry, 1991 , vol. 55, # 9 p. 2415 - 2416
反应条件
1: (i) LiAlH4, (ii) PBr3 2: ethanol 3: NaOH / methanol View Scheme
参考文献
Bhati,A.
Tetrahedron, 1962 , vol. 18, p. 1519 - 1526
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2 / diethyl ether 3: ethanol 4: HI, AcOH View Scheme
参考文献
Eiden; Meins
Archiv der Pharmazie, 1972 , vol. 305, # 2 p. 124 - 134
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2 / diethyl ether 3: ethanol 4: HI, AcOH 5: HCl View Scheme
参考文献
Eiden; Meins
Archiv der Pharmazie, 1972 , vol. 305, # 2 p. 124 - 134
反应条件
1: 94 percent / NH4OAc / acetic acid / 1.5 h / Heating View Scheme
参考文献
Bayardon, Jerome; Sinou, Denis
Synthesis, 2005 , # 3 art. no. Z19104SS, p. 425 - 428
反应条件
1: Na / Heating 2: (i) NaOMe, Et2O, (ii) /BRN= 506456/, Et2O, (iii) aq. H2SO4 View Scheme
参考文献
Hardegger,E. et al.
Helvetica Chimica Acta, 1963 , vol. 46, p. 2543 - 2551
参考文献
Seka; Fuchs
Monatshefte fuer Chemie, 1931 , vol. 57, p. 52,58
反应条件
1: sodium tetrahydroborate / methanol; tetrahydrofuran / 2.5 h / 70 °C 2: phosphorus tribromide / dichloromethane / 2 h / 20 °C 3: tetrahydrofuran / 1.5 h / -20 °C View Scheme
参考文献
Nuellen, Max P.; Goettlich, Richard
Synlett, 2013 , vol. 24, # 9 art. no. ST-2012-B1071-L, p. 1109 - 1112
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran 2: magnesium / tetrahydrofuran 3: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C 4: phosphoric acid / toluene / 5 h / Reflux View Scheme
参考文献
Jian, Yujuan; Sun, Gaojun; Li, Jiaming; Su, Dan; Li, Chuanrun; Zhong, Guochen
Chinese Journal of Chemistry, 2011 , vol. 29, # 7 p. 1423 - 1428
反应条件
1: 48 percent / AgI 2: 92 percent / aq. NaOH / methanol; ethanol / 1 h / 70 - 80 °C View Scheme
参考文献
Bringmann, Gerhard; Menche, Dirk; Muehlbacher, Joerg; Reichert, Matthias; Saito, Nozomi; Pfeiffer, Steven S.; Lipshutz, Bruce H.
Organic Letters, 2002 , vol. 4, # 17 p. 2833 - 2836
